Search results for "packed bed"
showing 10 items of 20 documents
Development of a Higee bioreactor (HBR) for production of polyhydroxyalkanoate: Hydrodynamics, gas–liquid mass transfer and fermentation studies
2010
Abstract This study addresses the hydrodynamics and mass transfer characterisation of a Higee bioreactor (HBR) for application to polyhydroxyalkanoate (PHA) production from Pseudomonas putida KT2442 fermentation. The motivation for this work is to address the potential oxygen transfer limitations which can severely impede the progress of this aerobic fermentation process and reduce PHA productivity in conventional bioreactors. It is shown that a maximum of 2.5 transfer units can be achieved in an oxygen-stripping operation where the presence of packing, higher rotor speeds, higher air flowrates and lower liquid flowrates all have a positive influence on the number of transfer units (NTU). W…
Liquid viscosity and flow rate effects on interfacial area in packed columns
1989
Abstract The influences of liquid kinematic viscosity and liquid flow rate on effective interfacial area for chemical absorption in a Raschig ring packed column were studied by absorbing carbon dioxide into potassium carbonate-bicarbonate-arsenite solutions. The viscosities of the absorbing liquid were varied by the addition of sugar. Analysis of the data shows that an increase in liquid flow rate increases the effective interfacial area over the whole viscosity range considered. The influence of liquid viscosity is more complex as the interfacial area increases with viscosity for low values, while decreasing at higher viscosities. Two correlations have been developed to express this behavi…
Etude numérique du comportement thermique d’un séchoir solaire utilisant un lit thermique pour le stockage d’énergie
2018
This thesis presents a numerical study of an indirect natural convection solar dryer for drying agricultural products (Figs). The first part analyzes a solar dryer containing a drying chamber coupled to a reversed absorber and a solar chimney. Simulations were made to determine the dynamic and thermal fields under the influence of the variation of the solar chimney configuration and the size of the inlet opening. The governing equations based on the standard k-ε turbulence model are solved by the finite volume method using the ANSYS-Fluent commercial code. The second part analyzes the effect of adding a thermal storage in the form of a gravel bed in the drying chamber. The bed is modeled as…
On-fibre solid-phase microextraction coupled to conventional liquid chromatography versus in-tube solid-phase microextraction coupled to capillary li…
2006
This paper compares the advantages and disadvantages of two different configurations for the extraction of triazines from water samples: (1) on-fibre solid-phase microextraction (SPME) coupled to conventional liquid chromatography (LC); and (2) in-tube SPME coupled to capillary LC. In-tube SPME has been effected either with a packed column or with an open capillary column. A critical evaluation of the main parameters affecting the performance of each method has been carried out in order to select the most suitable approach according to the requirements of the analysis. In the on-fibre SPME configuration the fibre coating was polydimethylsiloxane (PDMS)-divinylbenzene (DVB). The limits of de…
Experimental results on adsorption beds for air dehumidification
2016
Desiccant rotors are commonly used in large scale solar cooling open cycle applications. As is well known, adsorption heat sensibly reduces the dehumidification capacity of the desiccant material and results in lower system performance. The aim of this work is to describe an innovative solution that permits simultaneous mass and heat transfer. In particular, two components working with silica gel fixed beds were studied and compared. The first component is a simple packed bed containing silica gel grains. The second component is a fin and tube heat exchanger commonly used in several air conditioning applications wherein the spaces between the fins are filled with silica gel grains. In this …
Hydrodynamics of a cocurrent downflow of gas and foaming liquid through the packed bed. Part II. Liquid holdup and gas pressure drop
2003
Abstract In the present study the results of experiments have been presented whose aim was to determine the values of liquid holdup as well as gas pressure drop through the packing for systems foaming under the pulse flow regime. On the basis of 245 experimental points for the pulse flow regime the verification of the models describing the hydrodynamics of the system has been performed. Attention was focused on the models of Benkrid et al. (Chem. Eng. Sci. 52 (1997) 4021), Pina et al. (AIChE J. 47 (2001) 19) and Fourar et al. (Chem. Eng. Sci. 56 (2001) 5987). It has been concluded that none of the models analysed describes the hydrodynamics of the foaming systems with enough accuracy. Next,…
Triacylglycerol Analysis in Human Milk and Other Mammalian Species: Small-Scale Sample Preparation, Characterization, and Statistical Classification …
2015
In this work, a method for the separation of triacylglycerols (TAGs) present in human milk and from other mammalian species by reversed-phase high-performance liquid chromatography using a core–shell particle packed column with UV and evaporative light-scattering detectors is described. Under optimal conditions, a mobile phase containing acetonitrile/n-pentanol at 10 °C gave an excellent resolution among more than 50 TAG peaks. A small-scale method for fat extraction in these milks (particularly of interest for human milk samples) using minimal amounts of sample and reagents was also developed. The proposed extraction protocol and the traditional method were compared, giving similar results…
Towards the column bed stabilization of columns in capillary electroendosmotic chromatography
2000
This article discusses a novel method generating a continuous bed inside the CEC column. The column bed composed of microparticulate reversed-phase silica is completely immobilized by a hydrothermal treatment using water for the immobilization process. This process eliminates the manufacture of frits of both ends of the column and all problems associated with their preparation. Fundamental studies on operational parameters will be presented such as the dependence of the immobilization on the column temperature, the type of stationary phase and the column back pressure. The immobilized CEC columns show the same high column efficiency as packed columns with frits.
Modelling of the hydrodynamics of concurrent gas and liquid flow through packed bed
2016
The aim of the present study is to simulate concurrent gas and liquid flow through packed bed in the gas continuous flow regime (GCF) and continuity shock waves regime (CSW) using computational fluid dynamics (CFD). The application of multiple gas-liquid-solid model requires the knowledge of relationships determining interactions between phases. The exchange coefficients of these forces were defined by means of equations suggested by ATTOU et al. (1999). As a result of the computational simulation the following data were obtained: gas pressure drop in the bed, volume fraction distribution of a given phase (liquid and gas holdups) along the packing and its mean value in the reactor. The comp…
MODELING OF A TiO2-COATED QUARTZ -WOOL PACKED-BED PHOTOCATALYTIC REACTOR
2010
A fixed-bed, photocatalytic laboratory reactor aimed to degrade pollutants from water streams was designed and built. Quartz wool coated with a thin film of TiO2 was employed as the reactor filling. The photocatalyst was placed in the reactor forming a loose packing to guarantee the intimate contact among reactants, photons, and the photocatalytic surface. This reactor was employed to study the photocatalytic decomposition of a model pollutant (formic acid). A reactor–radiation–reaction model was developed, which was comprised of the reactor mass balance, radiation model, and kinetic model for the degradation of formic acid. The local superficial rate of photon absorption, which was necessa…